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Decagram-Scale Synthesis of N -{2-[4-(β- d -Glucopyranosyloxy)-2-methylphenyl]-1,1-dimethyl-2-oxoethyl}-3-methylthiophene-2-carboxamide (GPTC), a Metabolite of the Fungicide Isofetamid
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Publication Year
2023-09-07
Journal
Synlett
Publisher
Georg Thieme Verlag
Citation
Synlett, Vol.35 No.2, pp.221-224
Keyword
certified reference materialsGPTCisofetamidlarge-scale synthesis
All Science Classification Codes (ASJC)
Organic Chemistry
Abstract
A decagram-scale synthesis of N-{2-[4-(?-D-glucopyranosyloxy)-2-methylphenyl]-1,1-dimethyl-2-oxoethyl}-3-methylthiophene-2- carboxamide (GPTC), a metabolite of the fungicide isofetamid, has been achieved in a highly straightforward manner from the known compound 1-(4-hydroxy-2-methylphenyl)-2-methylpropan-1-one in eight steps with a 20% overall yield to provide a standard certified reference material for residue analysis in food.
ISSN
1437-2096
Language
eng
URI
https://aurora.ajou.ac.kr/handle/2018.oak/33703
https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=85172992895&origin=inward
DOI
https://doi.org/10.1055/a-2178-1442
Journal URL
https://www.thieme.de/de/synlett/journal-information-55964.htm
Type
Article
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Division of Pharmacy Sciences
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