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Effect of Al2O3 sandblasting particle size on the surface topography and residual compressive stresses of three different dental zirconia gradesoa mark
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Publication Year
2021-02-01
Publisher
MDPI AG
Citation
Materials, Vol.14, pp.1-19
Keyword
Air abrasionDental stress analysisPhase transitionSurface propertiesZirconium oxide
Mesh Keyword
Blasting conditionsConfocal laser microscopyMicro Raman SpectroscopyPartially stabilized zirconiaPeak shiftResidual compressive stressYttria stabilized tetragonal zirconias
All Science Classification Codes (ASJC)
Materials Science (all)
Abstract
This study investigated the effect of sandblasting particle size on the surface topography and compressive stresses of conventional zirconia (3 mol% yttria-stabilized tetragonal zirconia pol-ycrystal; 3Y-TZP) and two highly translucent zirconia (4 or 5 mol% partially stabilized zirconia; 4Y-PSZ or 5Y-PSZ). Plate-shaped zirconia specimens (14.0 × 14.0 × 1.0 mm3, n = 60 for each grade) were sandblasted using different Al2O3 sizes (25, 50, 90, 110, and 125 μm) under 0.2 MPa for 10 s/cm2 at a 10 mm distance and a 90° angle. The surface topography was characterized using a 3-D confocal laser microscopy and inspected with a scanning electron microscope. To assess residual stresses, the tetragonal peak shift at 147 cm−1 was traced using micro-Raman spectroscopy. Al2O3 sandblasting altered surface topographies (p < 0.05), although highly translucent zirconia showed more pro-nounced changes compared to conventional zirconia. 5Y-PSZ abraded with 110 μm sand showed the highest Sa value (0.76 ± 0.12 μm). Larger particle induced more compressive stresses for 3Y-TZP (p < 0.05), while only 25 μm sand induced residual stresses for 5Y-PSZ. Al2O3 sandblasting with 110 μm sand for 3Y-TZP, 90 μm sand for 4Y-PSZ, and 25 μm sand for 5Y-PSZ were considered as the recommended blasting conditions.
ISSN
1996-1944
Language
eng
URI
https://dspace.ajou.ac.kr/dev/handle/2018.oak/31821
DOI
https://doi.org/10.3390/ma14030610
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Type
Article
Funding
Funding: This work was supported by the National Research Foundation of Korea (NRF) grant funded by the Korea government (MSIT: Ministry of Science and ICT) (Grant No. NRF-2019R1F1A1062112) and this work was supported by the new faculty research fund of Ajou University School of Medicine (Grant No. M-2019-C0460-00040).
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Ahn, Byungmin  Image
Ahn, Byungmin 안병민
Department of Materials Science Engineering
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